Now showing 1 - 10 of 43
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Development and Performance Evaluation of a Portable Ceramic Water Filter with Exfoliated Graphite and Sawdust as an Additive

2024, Meraj Ahmad, Chandra Prakash, Arti Sharma, Dixit, Ambesh, Chhabra, Meenu, Plappally, Anand K

The availability of safe drinking water in non-networked rural areas and disaster-affected zones is dependent on point-of-use water filters. This study describes the design and performance assessment of a personal portable ceramic water filter named “sip-up.” Four sample variants were made using clay, exfoliated graphite (EG), and sawdust as raw materials. Samples were made using a mold to ensure uniformity and sintered at 850 °C. The experimental results showed that the sample containing the maximum amount of sawdust had the highest porosity of 36.07 ± 1.8%, providing an average flow rate of 0.61 ml/min in passive mode. The average pore size radius of all variants varied in the range of 1–10 nm, classifying the material as having a mesoporous structure. Compressive test results indicate that the addition of an organic additive (sawdust) decreases the compressive strength of filters as compared to non-organic additives. It has been observed that the addition of EG to clay does not significantly improve water filtration parameters as compared to samples containing only sawdust and clay. However, due to the smaller pore size, samples containing EG performed better in E. coli removal as compared to sawdust-containing samples. The final prototype can act as a single-use personal water filtration device that can be inserted into any commercial water bottle, making it an affordable and effective solution for hikers, travelers, and natural disasters such as floods and cyclones.

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Mixed-mode thermo-mechanical fracture: An adaptive multi-patch isogeometric phase-field cohesive zone model

2024, Zhanfei Si, Tiantang Yu, Weihua Fang, Sundararajan Natarajan, Hirshikesh

This work presents an adaptive phase-field cohesive zone model (PF-CZM) for simulating mixed-mode crack nucleation and growth in isotropic rock-like materials subjected to thermo-mechanical interactions. The proposed approach combines an adaptive multi-patch isogeometric analysis (MP-IGA) and length-scale insensitive PF-CZM. The formulation captures the distinct critical energy release rates for Mode-I and Mode-II fractures, which is crucial for predicting mixed-mode thermo-mechanical fracture behavior in isotropic rock-like materials. The PF-CZM governing equations are solved with isogeometric analysis based on locally refined non-uniform rational B-splines (LR NURBS), and the complex structural geometry is exactly described with multiple LR NURBS patches. The field variables, such as displacement, phase-field, and temperature at the interface of adjacent patches, are coupled using Nitsche's method. To enhance the computational efficiency while maintaining accuracy, a refinement-correction adaptive scheme combined with the structured mesh refinement strategy is developed. The proposed framework is validated against recent numerical and experimental results in the literature, particularly in the context of capturing complex behavior of mixed-mode crack propagation in isotropic rock-like materials subjected to thermo-mechanical loading.

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From Gaussian to lognormal: improving material property modeling for precise structural predictions

2024, R, Arun Kumar

Accurate prediction of material properties is essential in structural engineering design to ensure reliability and safety. Traditional approaches often rely on Gaussian distributions to model material variability. However, our research reveals limitations with Gaussian assumptions, particularly when covariance parameters exceed certain thresholds, leading to physically unrealistic negative values for material properties. To overcome these limitations, we investigate an alternative approach using lognormal distributions for material property modeling. Through Monte Carlo simulations employing Cholesky decomposition, we compare the performance of lognormal distributions with Gaussian counterparts. Our findings demonstrate that lognormal distributions offer a viable alternative, providing more accurate representations of material variability while maintaining computational efficiency. Furthermore, we utilize finite element method (FEM) data from Monte Carlo simulations to predict beam deflection using deep neural networks (DNNs). Leveraging inverse modeling techniques, we showcase the ability to predict elastic modulus from beam deflection data under both normal and lognormal distribution assumptions. By integrating lognormal modeling and inverse modeling techniques into structural analysis, we enhance the realism and accuracy of predictions, thereby improving reliability in engineering design. This paper discusses the implications of our findings and emphasizes the importance of considering alternative probability distributions for material property modeling in structural engineering applications.

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Low cost fabrication of continuous flow optofluidic microreactor for efficient dye degradation using graphene QDs@MOF (Ti) photocatalyst

2024, Gulshan Verma, Prashanth Venkatesan, Deblina Roy, Parthivi Aloni, Naresh Kumar Dega, Gupta, Ankur

The optofluidic microreactor, a convergence of optics and microfluidics, offers advanced functionalities that can be pivotal in the rapid assessment of nanocatalysts for tackling environmental contamination issues. This article presents an efficient approach for degrading Methylene blue (MB) dye, commonly used in the textile industry, within a cost-effective polydimethylsiloxane (PDMS) based continuous flow optofluidic microreactor. This microreactor combines graphene quantum dots (QDs) and NH2-MIL-125 (MOF(Ti)) as a highly effective photocatalyst coating within its microchannels. By directly incorporating graphene QDs@MOF(Ti) into the microchannels, the photocatalytic medium is brought into close proximity with the flowing MB dye solutions, thereby reducing the necessary interaction time and enhancing purification efficiency. Furthermore, the findings demonstrate an impressive degradation efficiency of ∼99% for MB dye at a flow rate of 50 μL min−1 under visible light irradiation, achieved in a single pass. Additionally, the microfluidic reactor exhibits prolonged stability of the photocatalyst, enabling its reuse without significant efficiency loss. In addition, a comparative analysis highlights the advantages of microreactor-based photocatalysis over traditional methods. These advancements in the features of the graphene QDs@MOF(Ti) nanocomposite substantiate their demonstrated superiority in degradation efficiency.

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Creep rupture study of dissimilar welded joints of P92 and 304L steels

2024, Gaurav Dak, Krishna Guguloth, R. S. Vidyarthy, Dariusz Fydrych, Pandey, Chandan

The present work investigates the high-temperature tensile and creep properties of the dissimilar metal weld joints of 304L austenitic stainless steel (SS) and P92 creep strength-enhanced ferritic-martensitic (CSEF/M) steel under different testing condition. Thermanit MTS 616 filler rod (P92 filler) and the multi-pass tungsten inert gas (TIG) welding process were used to create the dissimilar weld connection. The ultimate tensile strength (UTS) was evaluated in the temperature range of 450–850 °C. Creep testing was conducted at a temperature of 650 °C while applying stress levels of 130 MPa, 150 MPa, 180 MPa, and 200 MPa. The shortest creep life (2.53 h) was recorded for the specimen tested at 650 °C and subjected to 200 MPa, whereas the longest creep life (~ 242 h) was observed for the specimen tested at 650 °C with a stress of 130 MPa. The linear regression model was developed using an applied stress (σ) v/s rupture time (tR) plot at 650 °C. The applied stress and rupture time followed the logarithmic equation: log(tR) = 22.57566 + (-9.55294) log (σ). The detailed microstructural characterization and micro-hardness distribution across the fractured specimens was carried out. The findings demonstrated that the service life span of this weld joint at high temperature and stress conditions is influenced by the undesired microstructural changes at elevated temperature, such as coarsening of the precipitates, development of the Laves phase, softening of the matrix, and strain-ageing phenomenon.

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Role of Microstructure Evolution During Welding on Mechanical Properties and Residual Stresses of the Inconel 718 and Austenitic Stainless Steel 304L Dissimilar Weld Joint

2024, Niraj Kumar, Prakash Kumar, Ravi Shanker Vidyarthy, Pandey, Chandan

For this study, the researchers aimed to dissimilar weld the Nickel-based superalloy Inconel 718 (IN 718) with austenitic stainless steel 304L (ASS 304L) using the gas tungsten arc welding (GTAW) technique and Nickel-based filler IN 82 (ERNiCr-3). In order to examine the weld microstructures, we utilized optical microscopy (OM) and field emission scanning electron microscopy (FESEM) with energy-dispersive spectroscopy (EDS) to identify any segregation present in various weld zones. Through optical and FESEM analyses, it was revealed that the base metals (BM) exhibit an austenitic character. The IN 718 BM matrix contains dispersed γ′ and γ″ strengthening precipitates within the Nickel matrix. On the other hand, the ASS 304L BM displayed a unique austenitic microstructure characterized by twins features. The weld metal exhibited solidification grain boundaries (SGBs), migrated grain boundaries (MGBs), and distinct dendritic microstructures that had an impact on the properties of the weld. Through extensive analysis and mapping of the IN 82 weld zone, it was discovered that interdendritic regions contain carbides of Nb, Cr, and Ti. In addition, there were Unmixed zone (UZ) areas between the IN 82 filler and the base materials on both sides of the weld zone, appearing as islands and beaches. The texture of the different weld zones was evaluated using electron backscattered diffraction (EBSD) analysis. Additionally, the presence of a notable level of strain within the weld metal grains was observed through Kernel average misorientation (KAM) micrographs. Fractures were observed in the IN 82 weld zone, indicating that it is the weakest area in the IN 718/ASS 304L dissimilar weld at room temperature, according to the outputs of the tensile tests. The micro-hardness profile showed substantial hardness values in the weld zone, which can be attributed to the appearance of a diverse microstructure and additional precipitates. At room temperature, the recorded average tensile strength of the dissimilar weld joint was 626 MPa. In addition, experiments were carried out at high temperatures of 550 °C, 600 °C, and 650 °C to measure the tensile strength. In the high-temperature tensile tests, it was observed that the IN 82 weld zone exhibited higher tensile strength compared to the ASS 304L BM. Interestingly, the high temperatures tensile specimens failed in the 304L BM. The Charpy impact toughness test was performed with notches at ASS 304L HAZ, IN 718 HAZ, and the weld center. Using the deep hole drilling (DHD) technique, we were able to quantify residual stress and identify the location of the highest tensile residual stress, which was found to be 3 mm from the weld surface. (Figure presented.)

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Corrosion performance of super duplex stainless steel and pipeline steel dissimilar welded joints: a comprehensive investigation for marine structures

2024, Anup Kumar Maurya, Shailesh M. Pandey, Chhibber, Rahul, Dariusz Fydrych, Pandey, Chandan

This study investigates the corrosion behavior of dissimilar gas tungsten arc (GTA) welded joints between super duplex stainless steel (sDSS 2507) and pipeline steel (X-70) using electrochemical and immersion corrosion tests. The GTA welds were fabricated using ER2594 and ER309L filler metals. The study examined the electrochemical characteristics and continuous corrosion behavior of samples extracted from various zones of the weldments in a 3.5 wt.% NaCl solution, employing electrochemical impedance spectroscopy, potentiodynamic polarization methods, and an immersion corrosion test. EIS and immersion investigations revealed pitting corrosion in the X-70 base metal/X-70 heat-affected zone, indicating inferior overall corrosion resistance due to galvanic coupling. The corrosion byproducts identified in complete immersion comprised α-FeOOH, γ-FeOOH, Fe3O4, and Fe2O3, whereas γ-FeOOH and Fe3O4 were predominant in dry/wet cyclic conditions. Corrosion escalated with dry/wet cycle conditions while maintaining a lower level in complete immersion. The corrosion mechanism involves three wet surface stages in dry/wet cycles and typical oxygen absorption during complete immersion. Proposed corrosion models highlight the influence of Cl−, O2, and rust layers.

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Fatigue crack growth in functionally graded materials using an adaptive phase field method with cycle jump scheme

2024, S. Natarajan, Ean Tat Ooi, Hirshikesh

Functionally graded materials provide versatility in adjusting the volume fractions of constituent materials to meet specific design requirements. However, this customization often introduces mode-mixity at the crack tip, posing challenges in predicting fracture under cyclic loading with discrete approaches and computationally expensive with conventional phase-field fracture models. To address these issues, this paper introduces an adaptive phase-field fracture formulation with cycle jump scheme to elegantly predict fatigue crack nucleation and growth in functionally graded materials. Within this framework, the effective properties at a point are estimated using the Mori–Tanaka homogenization scheme, while the crack growth due to cyclic load is captured by incorporating an additional fatigue degradation parameter. Moreover, the computational efficiency of the proposed framework is improved through an adaptive mesh refinement and explicit cycle jump scheme. The adaptive refinement scheme utilizes an error indicator derived from both the displacement solution and phase-field variable. The adaptive refinement scheme is integrated with efficient quadtree decomposition, which generates a hierarchical mesh structure. Hanging nodes resulting from the quadtree decomposition are efficiently handled using a polygonal finite element method. The proposed framework is validated against experimental and numerical results reported in the literature. Furthermore, we investigate the fatigue crack growth resistance across a broad range of material gradation directions, gaining valuable insights and identifying functionally graded materials with high fatigue resistance.

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Flash evaporation in a superheated liquid pool using water as medium

2024, Sarvjeet Singh, Kothadia, Hardikkumar Bhupendra, Chakraborty, Prodyut Ranjan

This paper proposes a fast cooling technology called flash evaporation or flashing to overcome cooling problems. Flashing is a pressure-driven phase change phenomenon widely studied because of its complex physics and numerous applications. An experimental system is fabricated to study the efficiency of the proposed process by considering water as a working fluid. A transparent acrylic column is used as the flash chamber, enabled with a high-speed camera to visualize and capture this fast and complex process. Experiments have been carried out with various initial temperatures from 65 °C to 80 °C, initial vacuum tank pressure ranging from 11.32 kPa to 41.32 kPa, and initial water heights of 80 mm and 140 mm. The flashing phenomenon is divided into two stages based on its effectiveness. From the present study, it becomes apparent that the drop in the temperature increases with the initial temperature and decreases with increasing vacuum tank pressure. The cooling rate is improved by 49.1% by increasing the initial pool temperature by 23%. The present study demonstrates an effective application of the flashing process in areas requiring high cooling rates and rapid vapour generation, such as refrigeration and drying.

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Influence of filler materials on GTAW dissimilar welds: Inconel 718 and austenitic stainless steel 304L

2024, Niraj Kumar, Prakash Kumar, Pandey, Chandan

The investigation carried out in the current study illustrates the dissimilar gas tungsten arc welding (GTAW) between Inconel 718 (IN 718) and austenitic stainless steel (ASS 304L) utilizing three different filler materials. This study utilizes Ni-based fillers (ERNiCrCoMo-1 (IN 617) and ERNiFeCr-2 (IN 718)), and austenitic filler ASS 304L and characterizes the relationship among microstructural and mechanical characteristics using identical weld parameters. The obtained dissimilar weld joint using Ni-based filler materials depicts no weld solidification cracking, whereas austenitic filler causes the weld solidification cracks. The microstructural characterizations were examined using optical and FESEM revealing the occurrence of columnar, cellular, and equiaxed dendritic structures in all three weld metals. FESEM/EDS analysis illustrates the occurrence of Mo and Cr-rich phases (M23C6 and Mo6C) in ERNiCrCoMo-1 weld metal, NbC, Mo/Ti–rich, and laves phases in ERNiFeCr- 2 weld metal and Cr- rich carbides in ASS 304L weld metals. EBSD assessment shows the improved texture of the weld metals through IPF and PF maps. The Vickers microhardness demonstrates the highest hardness value (271 HV5) for the ERNiFeCr- 2 weld metal due to the existence of the brittle intermetallic phases, and minimum in the case of ASS 304L weld metals (156 HV5). The ambient temperature tensile test exhibits the maximum (649 MPa) and minimum (404 MPa) UTS corresponding to ERNiCrCoMo-1 and ASS 304L weld metals respectively. The tensile specimens for all the weld metals experience fracture from the weld metals. The Charpy toughness values of the weld metals show lower values (ERNiCrCoMo-1 (70 J), ERNiFeCr-2 (56 J) and ASS 304L (32 J)) than the BMs (IN 718 (135 J) and ASS 304L (228 J). Residual stress analysis was conducted employing the deep hole drilling (DHD) technique, indicating that the highest residual stress occurs 2 mm below the top weld face, classified as tensile stress for all three used filler materials.